Method of synthesis of 17β-hydroxy-11β-[4-(dimethylamino)-phenyl]-17α-(prop-1-ynyl)-estra-4,9-diene-one
DOI Number:
Reaction Category:
MOP ID:
MOP_0000671
Educt:
tert-butyldimethyl(((8S,13S,14S,17S)-13-methyl-17-(prop-1-yn-1-yl)-1,2,4,6,7,8,12,13,14,15,16,17-dodecahydrospiro[cyclopenta[a]phenanthrene-3,2'-[1,3]dioxolan]-17-yl)oxy)silane, hydrogen peroxide
Product:
tert-butyldimethyl(((5'R,8'S,10'R,13'S,14'S,17'S)-13'-methyl-17'-(prop-1-yn-1-yl)-1',2',7',8',12',13',14',15',16',17'-decahydro-4'H,6'H-spiro[[1,3]dioxolane-2,3'-[5,10]epoxycyclopenta[a]phenanthren]-17'-yl)oxy)silane
Catalyst:
(8α,9R)-9-hydroxy-6′-methoxy-1-(phenylmethyl)-cinchonanium bromide
Cas No:
69212-47-1
Associated Product from Buchler GmbH:
Quinine Base
Cas No:
130-95-0