A quinine squaramide catalyzed enantioselective [4+2] cycloaddition between ortho-hydroxyphenyl para-quinone methide and γ-butenolides for preparation of chiral 3,4-dihydrocoumarins.

DOI Number:

10.1016/j.tetlet.2024.155311

Reaction Category:

MOP ID:

MOP_0000565

Educt:

γ-butenolides, ortho-hydroxyphenyl para-quinone methide

Product:

(3S,4S)-3-(2-(4-chlorophenyl)-2-oxoethyl)-4-(3,5-di-tert-butyl-4-hydroxyphenyl)chroman-2-one

Catalyst:

3-[[[3,5-Bis(trifluoromethyl)phenyl]methyl]amino]-4-[[(8α,9S)-6′-methoxycinchonan-9-yl]amino]-3-Cyclobutene-1,2-dione

Cas No:

1210360-60-3

Associated Product from Buchler GmbH:

3-[[[3,5-Bis(trifluoromethyl)phenyl]methyl]amino]-4-[[(8α,9S)-6′-methoxycinchonan-9-yl]amino]-3-Cyclobutene-1,2-dione

Cas No:

1210360-60-3