Observation of neighboring ortho-hydroxyl group participation in organocatalytic asymmetric sequential Michael-lactonization reactions: synthesis of highly substituted chiral spirodihydrocoumarins.

DOI Number:

10.1039/C2OB07122C

Reaction Category:

RXNO ID:

RXNO_0000009

Educt:

substituted (E)-2-(2-nitrovinyl)phenol, 2-oxocyclopentane-1-carboxylates

Product:

spirodihydrocoumarins, (9R,9aS)-9-(nitromethyl)-1,2-dihydrocyclopenta[b]chromene-9a(9H)-carboxylates

Catalyst:

N-[3,5-Bis(trifluoromethyl)phenyl]-N′-[(8α,9S)-6′-methoxycinchonan-9-yl]thiourea

Cas No:

852913-16-7

Associated Product from Buchler GmbH:

N-[3,5-Bis(trifluoromethyl)phenyl]-N′-[(8α,9S)-6′-methoxycinchonan-9-yl]thiourea

Cas No:

852913-16-7